RAPID-DETERMINATION OF 4-VINYL GUAIACOL AND FERULIC ACID IN BEERS ANDWORTS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

Citation
D. Madigan et al., RAPID-DETERMINATION OF 4-VINYL GUAIACOL AND FERULIC ACID IN BEERS ANDWORTS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY, Journal of the American Society of Brewing Chemists, 52(4), 1994, pp. 152-155
Citations number
16
Categorie Soggetti
Biothechnology & Applied Migrobiology","Food Science & Tenology
ISSN journal
03610470
Volume
52
Issue
4
Year of publication
1994
Pages
152 - 155
Database
ISI
SICI code
0361-0470(1994)52:4<152:RO4GAF>2.0.ZU;2-O
Abstract
Sensitive methods for the determination of ferulic acid and 4-vinyl gu aiacol in beers and worts are described. Samples were analyzed by dire ct-injection high-performance liquid chromatography using an octadecyl silica column. Detection was by either fluorescence monitoring (for 4 -vinyl guaiacol alone) or electrochemical detection (for simultaneous determination of ferulic acid and 4-vinyl guaiacol). The methods were applied mainly to the analysis of production beers but were used also to monitor the decarboxylation of ferulic acid to 4-vinyl guaiacol in wort during a small-scale fermentation deliberately contaminated with a wild yeast strain.