THE EFFECT OF CONTROLLED IMPURITY INCORPORATION ON INTERFACIAL ROUGHNESS IN GAAS ALXGA1-XAS SUPERLATTICE STRUCTURES GROWN BY METALORGANIC VAPOR-PHASE EPITAXY/
Jm. Redwing et al., THE EFFECT OF CONTROLLED IMPURITY INCORPORATION ON INTERFACIAL ROUGHNESS IN GAAS ALXGA1-XAS SUPERLATTICE STRUCTURES GROWN BY METALORGANIC VAPOR-PHASE EPITAXY/, Journal of crystal growth, 145(1-4), 1994, pp. 792-798
Oxygen impurities are known to degrade the bulk and heterointerfacial
quality of AlxGa1-xAs/GaAs layers grown by metalorganic vapor phase ep
itaxy (MOVPE). We have intentionally added oxygen at the interfaces of
Al0.3Ga0.7As/GaAs superlattice layers to examine its effect on interf
acial and surface roughness in these structures. Small angle X-ray dif
fraction and atomic force microscopy (AFM) were used to quantify and c
ompare both small scale interfacial roughness and large scale surface
roughness. Interfacial oxygen incorporation was found to increase with
increasing substrate misorientation angle off (100) toward the (110)
and this was reflected in increased interfacial roughness. Large scale
surface structures with spacings of similar to 2.0 mu m were observed
using AFM for growth on nominally (100) substrates. The existence of
these features is also indicated in X-ray correlated roughness measure
ments. A mechanism of preferential oxygen incorporation at surface ste
p edges is proposed to explain the evolution of roughness in the super
lattice layers.