Gr. Lai et al., DEPOSITION OF DIAMOND FILMS IN A CLOSED HOT-FILAMENT CVD SYSTEM, Journal of research of the National Institute of Standards and Technology, 100(1), 1995, pp. 43-49
A closed system hot filament chemical vapor deposition (CVD) reactor h
as been used to deposit diamond films on silicon substrates. A fixed c
harge of hydrogen gas is fed into the deposition system until the desi
red deposition pressure level is reached. A solid graphite cylindrical
rod held above the tungsten filament was the carbon source. System pa
rameters for diamond film growth have been determined. The diamond str
ucture of the films has been verified by x-ray diffraction (XRD). Morp
hology typical of CVD diamond films has been observed in scanning elec
tron microscopy (SEM). The quality of the diamond films has been evalu
ated by micro-Raman spectroscopy.