Tm. Cheng et al., FORMATION AND CHARACTERIZATION OF GAAS AS SUPERLATTICE GROWN BY MOLECULAR-BEAM EPITAXY AT LOW SUBSTRATE-TEMPERATURE/, Journal of crystal growth, 150(1-4), 1995, pp. 28-32
High-resolution X-ray diffractometer and transmission electron microsc
ope (TEM) are used to characterize the redistribution of As precipitat
es in Si delta-doped GaAs grown by molecular beam epitaxy at low subst
rate temperature (230 degrees C). The superlattice satellite peaks are
observed for samples annealed at 700-800 degrees C for 10 min, which
is attributed to the formation of a GaAs/As superlattice during the an
nealing period. The degree of As precipitates confined on the delta-do
ped planes is revealed on the intensity of satellite peaks in the X-ra
y rocking curves, as confirmed by the TEM observations. The lattice ex
pansion and contraction of the annealed low-temperature epitaxial laye
rs can be easily observed from the asymmetry of the satellite peaks.