POROSITY OF SHAPES FROM HYDROTHERMALLY TREATED TITANIA

Citation
B. Rohlkuhn et al., POROSITY OF SHAPES FROM HYDROTHERMALLY TREATED TITANIA, Mikrochimica acta, 125(1-4), 1997, pp. 21-24
Citations number
10
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00263672
Volume
125
Issue
1-4
Year of publication
1997
Pages
21 - 24
Database
ISI
SICI code
0026-3672(1997)125:1-4<21:POSFHT>2.0.ZU;2-0
Abstract
Titania nanopowders obtained by hydrolysis of titanium alkoxides and c onsecutive hydrothermal treatment were compacted and sintered. The inf luence of preparation conditions (alkyl, pH of hydrolysis, temperature of hydrothermal treatment, compacting pressure, sintering temperature ) on the porosity of powders, compacts and sintered bodies was investi gated by nitrogen sorption and mercury intrusion. Optimum conditions a re derived to prepare high-density ceramics at relatively low sinterin g temperature.