O. Nishiyama et al., ANALYSIS OF PRESERVATIVES IN FOODS BY USING STEAM DISTILLATION WITH AMMONIUM-SULFATE SATURATED SOLUTION, Shokuhin Eiseigaku Zasshi, 36(4), 1995, pp. 495-500
A method for the analysis of preservatives in foods by using steam dis
tillation with saturated ammonium sulfate was developed. As the ammoni
um sulfate saturated solution was brought to pH 2 with phosphoric acid
, so simultaneous distillation of benzoic acid (BA), sorbic acid (SoA)
, dehydroacetic acid (DHA), p-hydroxybenzoic acid esters (PHBA-Es) and
propionic acid (PA) was possible. Recoveries of BA ranged from 89.3 t
o 101.4%, SoA from, 96.3 to 100.8%, DHA from 82.3 to 95.4%, PHBA-Es fr
om 84.7 to 103.5%, and PA from 96.7 to 100.8%.