The new approach to enhancing the selectivity of sorption separation o
f metal ions was suggested. The approach is based on using mixed sorbe
nts, which may be obtained, e.g. by simultaneous immobilization of com
plexing reagents on silica gel and reverse-phase silica gel (C-16, Ph)
. The methods are developed for the simultaneous determination of two
(Co-Fe, Co-Zn, Al-Mn) or three (Al, Mn and Fe) elements in the concent
ration range 2.10(-6)-7.10(-4) M with the performance of 21-36 samples
per hour.