Nr. Antoniosi et al., FAST QUANTITATIVE-ANALYSIS OF SOYBEAN OIL IN OLIVE OIL BY HIGH-TEMPERATURE CAPILLARY GAS-CHROMATOGRAPHY, Journal of the American Oil Chemists' Society, 70(10), 1993, pp. 1051-1053
Analysis of glycerides has always been of great interest. especially t
o the food industry. Several methods have been developed, and attempts
to improve analytical conditions are prevalent. Among these methods,
high-temperature capillary gas chromatography has received particular
consideration because it rapidly provides a glyceride profile. In this
paper, we discuss a method to identify and quantitate mixtures of oli
ve and soybean oils with the intention of verifying the latter as an a
dulterant of olive oils. The contamination of olive oil with soybean o
il was detected by the presence of the triglyceride trilinolein, which
does not exist in pure olive oil, although it is abundant in soybean
oil. A calibration curve was constructed with several levels of contam
ination, and the lowest amount of detectable soybean oil was determine
d to be 4%.