A MIRROR FURNACE FOR NEUTRON-DIFFRACTION UP TO 2300-K

Citation
G. Lorenz et al., A MIRROR FURNACE FOR NEUTRON-DIFFRACTION UP TO 2300-K, Journal of applied crystallography, 26, 1993, pp. 632-635
Citations number
21
Categorie Soggetti
Crystallography
ISSN journal
00218898
Volume
26
Year of publication
1993
Part
5
Pages
632 - 635
Database
ISI
SICI code
0021-8898(1993)26:<632:AMFFNU>2.0.ZU;2-Z
Abstract
This paper describes a mirror furnace that has been developed for neut ron diffraction work at temperatures up to 2300 K. It is based on a re flecting rotational ellipsoid, in which the heating element, a halogen lamp, is placed at one focus and the sample at the other. It works in a normal, i.e. oxidizing, atmosphere, but can also be used in a vacuu m. It has been developed for experiments of long duration. The stabili ty and reproducibility of the temperature are better than 1% of the se tting temperature. Further main characteristics are applicability to s ingle-crystal and powder work, very low background, low power consumpt ion and very easy and cheap handling. Several experiments have been ca rried out with the furnace.