ERROR ANALYSIS OF CRYSTALLINE PTYCHOGRAPHY IN THE STEM MODE

Citation
Bc. Mccallum et Jm. Rodenburg, ERROR ANALYSIS OF CRYSTALLINE PTYCHOGRAPHY IN THE STEM MODE, Ultramicroscopy, 52(1), 1993, pp. 85-99
Citations number
12
Categorie Soggetti
Microscopy
Journal title
ISSN journal
03043991
Volume
52
Issue
1
Year of publication
1993
Pages
85 - 99
Database
ISI
SICI code
0304-3991(1993)52:1<85:EAOCPI>2.0.ZU;2-5
Abstract
We analyse errors associated with ptychographical phase determination of coherent convergent beam electron diffraction (CBED) patterns. The basis of this method is to observe the CBED patterns, as the probe is scanned across the specimen, in the regions where diffracted orders ov erlap, and measure the phases of the resulting sinusoidal intensity va riations in such regions. The method is shown to be insensitive to the objective lens transfer function (i.e. to defocus, astigmatism and al ignment), the degree of spatial coherence, specimen drift, and errors in probe scan rate. The robustness of this technique is confirmed by p resenting results of its application to data recorded from an optical analogue of a scanning transmission electron microscope.