M. Komath et al., PREPARATION OF GAMMA-NICKEL OXYHYDROXIDE THROUGH HIGH-TEMPERATURE REACTION OF NICKEL WITH ANHYDROUS SODIUM-HYDROXIDE, Materials chemistry and physics, 36(1-2), 1993, pp. 190-193
Gamma-nickel oxyhydroxide (gamma-NiOOH) was prepared from the reaction
of nickel with NaOH at similar to 850 degrees C. The reaction product
s were separated by leaching with water after the system was cooled. T
he product, characterized by transmission electron microscopy, X-ray d
iffractometry, infrared and thermogravimetric methods, was found to be
gamma-NiOOH.