H. Heinke et al., RELAXATION AND MOSAICITY PROFILES IN EPITAXIAL LAYERS STUDIED BY HIGH-RESOLUTION X-RAY-DIFFRACTION, Journal of crystal growth, 135(1-2), 1994, pp. 41-52
A novel nondestructive method correlating the strain gradient in parti
ally relaxed epilayers with a profile of crystalline mosaicity is demo
nstrated by using high resolution X-ray diffraction. By reciprocal spa
ce mapping, a distribution of the scattered intensity near reciprocal
lattice points was found, which is characteristic for partially relaxe
d layers. This distribution is described by a relaxation-mosaicity tri
angle which is modified in a characteristic way for different reflecti
on orders. The increase in mosaicity with progressive relaxation is qu
antified from diffraction profiles recorded along selected directions
in reciprocal space. The determination of the depth profile of strain
implies also the knowledge of the depth gradient of the mosaicity. The
method is demonstrated for a partially relaxed ZnSe layer grown by MB
E on (001) GaAs.