Ty. Chiang et al., LOW-TEMPERATURE GAAS EPITAXIAL-GROWTH ON SI(100) BY MOLECULAR-BEAM EPITAXY AND THE POSTGROWTH RAPID THERMAL ANNEALING, Journal of crystal growth, 135(3-4), 1994, pp. 469-475
This article presents low temperature GaAs epitaxial growth on Si(100)
by molecular beam epitaxy and the improvement of epitaxial quality by
post-growth rapid thermal annealing. The silicon wafer was ex-situ cl
eaned by spin-etch method to obtain a hydrogen-passivated surface befo
re wafer loading. An in-situ cleaning process for hydrogen removal was
carried out in the growth chamber by heating the silicon substrate to
a low pre-growth desorption temperature (250-600-degrees-C) prior to
epitaxial growth. Epitaxial films were grown at 250-580-degrees-C with
strained layer superlattice to reduce defect density. The epitaxial f
ilms were characterized by cross-sectional transmission electron micro
scopy, scanning electron microscopy, photoluminescence, and double cry
stal X-ray diffraction. The GaAs epitaxial quality improves with pre-g
rowth desorption temperature and deposition temperature. The epitaxial
films were treated by rapid thermal annealing to improve epitaxial qu
ality. Optimum annealing conditions of epitaxial films grown at differ
ent temperature were also investigated.