M. Kittler et J. Larz, ANALYTICAL, STRUCTURAL AND ELECTRICAL CHARACTERIZATION OF SIGE LAYERSBY ELECTRON MICROBEAM TECHNIQUES, Mikrochimica acta, 114, 1994, pp. 327-333
k-ratios of Ge-L(alpha) and Si-K(alpha) measured at different beam ene
rgies allow to evaluate simultaneously composition and thickness of Si
Ge layers on a Si substrate. A simple technique applying backscattered
electrons also enables estimation of composition of bulk SiGe and of
composition and thickness of relatively thick (approximately 200 nm) S
iGe layers on Si. Electron channeling patterns of pseudomorphic SiGe/S
i structures and of pure Si substrate show no significant differences
whereas in relaxed structures a smearing of the pattern with increasin
g density of misfit dislocations is observed. Under particular conditi
ons the technique of the electron beam induced current permits imaging
of recombination-active misfit dislocations with a spatial resolution
around 0.2 mum. Moreover, a repulsion of holes due to the valence-ban
d offset in a n-Si/SiGe heterostructure was detected.