SPATIAL-RESOLUTION IN SELECTED-AREA EELS

Citation
M. Schenner et P. Schattschneider, SPATIAL-RESOLUTION IN SELECTED-AREA EELS, Ultramicroscopy, 55(1), 1994, pp. 31-41
Citations number
21
Categorie Soggetti
Microscopy
Journal title
ISSN journal
03043991
Volume
55
Issue
1
Year of publication
1994
Pages
31 - 41
Database
ISI
SICI code
0304-3991(1994)55:1<31:SISE>2.0.ZU;2-8
Abstract
We investigate the effect of objective-lens chromatic aberration on qu antitative chemical microanalysis using electron energy-loss spectrome try in the electron microscope. Experimental tests were done on a spec imen with a planar interface under the condition of a rather large chr omatic error in image mode. We discuss three different models of image formation with inelastically scattered electrons. Simulations for Ni show that the quantum-mechanical image theory for large defocus values is practically equivalent to a Lorentzian image distribution and desc ribes the experimental data satisfactorily. A method to obtain a prope r defocus setting for the compensation of the chromatic error is also presented.