SOME NOTES ON THE SELECTION OF STRUCTURAL CHIRALITY BY CBED

Citation
Aws. Johnson et Ar. Preston, SOME NOTES ON THE SELECTION OF STRUCTURAL CHIRALITY BY CBED, Ultramicroscopy, 55(3), 1994, pp. 348-355
Citations number
14
Categorie Soggetti
Microscopy
Journal title
ISSN journal
03043991
Volume
55
Issue
3
Year of publication
1994
Pages
348 - 355
Database
ISI
SICI code
0304-3991(1994)55:3<348:SNOTSO>2.0.ZU;2-2
Abstract
A simple experimental indication of the Fourier coefficients which are sensitive to hand is given in CBED patterns by those non-zero Laue zo ne reflections which clearly break a mirror line that is present in th e zero Laue zone. It has been found possible to determine the chiralit y of thin crystals of Ho2Ge2O7 and of Bi12GeO24 by interpreting the re lative intensity of such reflections with a three-beam calculation. Mu ltislice calculations which matched the experimental patterns gave the same chirality. It is found that projections which contain mirrors ar e the most practical to use since they can be easily aligned.