THE EFFECT OF THE SHAPE FUNCTION ON SMALL-ANGLE SCATTERING ANALYSIS BY THE MAXIMUM-ENTROPY METHOD

Citation
Pr. Jemian et Aj. Allen, THE EFFECT OF THE SHAPE FUNCTION ON SMALL-ANGLE SCATTERING ANALYSIS BY THE MAXIMUM-ENTROPY METHOD, Journal of applied crystallography, 27, 1994, pp. 693-702
Citations number
31
Categorie Soggetti
Crystallography
ISSN journal
00218898
Volume
27
Year of publication
1994
Part
5
Pages
693 - 702
Database
ISI
SICI code
0021-8898(1994)27:<693:TEOTSF>2.0.ZU;2-6
Abstract
Analysis of small-angle scattering data to obtain a particle-size dist ribution is dependent upon the shape function used to model the scatte ring. From a maximum-entropy analysis of small-angle scattering data, the effect of shape-function selection on the obtained size distributi on is demonstrated using three different shape functions to describe t he same scattering data from each of two alloys. The alloys have been revealed by electron microscopy to contain a distribution of randomly oriented and mainly noninteracting irregular ellipsoidal precipitates. A comparison is made between the different forms of the shape functio n. The effect of an incident-wavelength distribution is also shown. Th e importance of testing appropriate shape functions and validating the se against other microstructural studies is discussed.