OPTIMAL CONDITIONS FOR FRACTIONATION OF RAPESEED LECITHIN WITH ALCOHOLS

Authors
Citation
M. Sosada, OPTIMAL CONDITIONS FOR FRACTIONATION OF RAPESEED LECITHIN WITH ALCOHOLS, Journal of the American Oil Chemists' Society, 70(4), 1993, pp. 405-410
Citations number
11
ISSN journal
0003021X
Volume
70
Issue
4
Year of publication
1993
Pages
405 - 410
Database
ISI
SICI code
0003-021X(1993)70:4<405:OCFFOR>2.0.ZU;2-9
Abstract
Deoiled rapeseed lecithin was fractionated with ethanol, and optimum c onditions have been determined to improve purified lecithin yield and phosphatidylcholine (PC) enrichment. The effect of extraction time, so lvent volume, ethanol concentration and temperature on the yield and t he PC enrichment have been described in the form of regression equatio ns. A full factorial experiment method and a second-order orthogonal d esign were used in the study. 'rhe regression equations were calculate d for the maximum value of the response functions optimized by an elec tronic data processing method, and the results (yield and PC enrichmen t calculated from regression equations) were compared with those obtai ned in control experiments. The use of calculated optimal parameters i n the fractionation process led to 81-96% and 58% increments in yield and PC enrichment, respectively.