An ultrasonic vibration aided etching technique for revealing dislocat
ions in GaAs has been developed. This technique, which employs CrO3-HF
aqueous solutions aided by ultrasonic vibration, produces clear etch
pit patterns in thinly etched layers of GaAs, without light irradiatio
n and agitation, at room temperature. Therefore, this technique is sui
table to reveal dislocations in epitaxial layers of GaAs.