Pp. Buaud et al., A STUDY OF SILICON EPITAXIAL-GROWTH ON SILICON SUBSTRATES EXPOSED TO AR ELECTRON-CYCLOTRON-RESONANCE PLASMAS, Journal of vacuum science & technology. B, Microelectronics and nanometer structures processing, measurement and phenomena, 13(4), 1995, pp. 1442-1446
Epitaxial growth of Si on Si(100) wafers was carried out at 700 degree
s C in an Ar microwave electron cyclotron resonance plasma chemical va
por deposition system. Both plasma exposure prior to growth and epitax
ial growth were monitored by real-time single-wavelength ellipsometry,
first to determine an optimum end point for Ar plasma cleaning which
would favor quality epitaxial growth, and second to follow the growth
of the epitaxial film. Spectroscopic ellipsometry combined with cross-
sectional transmission electron microscopy and atomic force microscopy
were used to characterize the epitaxial films, the epitaxial film/sub
strate interface, and the surface morphology. Secondary-ion mass spect
roscopy was used to evaluate the contamination levels st the film/subs
trate interface. Epitaxial films were successfully grown on both, smoo
th and rough (20-30 nm roughness layer) Si substrates. For both cases
the top surface of the epitaxial film was smooth, but the interfaces w
ere different. (C) 1995 American Vacuum Society.