H. Amenitsch et al., PERFORMANCE AND FIRST RESULTS OF THE ELETTRA HIGH-FLUX BEAMLINE FOR SMALL-ANGLE X-RAY-SCATTERING, Journal of applied crystallography, 30(2), 1997, pp. 872-876
A new beamline for small-angle X-ray scattering (SAXS) has recently be
en constructed and is presently under final commissioning at the 2 GeV
storage ring ELETTRA. It has been designed specifically for time-reso
lved studies of non-crystalline and fibrous materials and has been opt
imized for small-angle scattering measurements. The beamline operates
with a SAXS resolution between 10 and about 1400 Angstrom in d spacing
(at 8 keV) and has been optimized with respect to high flux at the sa
mple [of the order of 10(13) photons s(-1) for 8 keV photons (2 GeV, 4
00 mA)]. Soon it will be possible to perform simultaneously wide-angle
diffraction measurements in the d-spacing range 1.2-8 Angstrom (at 8
keV). In order to allow time-resolved (resolution similar to 1 ms) sma
ll-angle scattering measurements, a high-power 57-pole wiggler is used
as the beamline source. From its beam, one of three discrete energies
, 5.4, 8 and 16 keV, can be selected with a double-crystal monochromat
or, which contains three pairs of asymmetrically cut plane Si(111) cry
stals. Downstream, the beam is focused horizontally and vertically by
a toroidal mirror. Commissioning tests of this new SAXS beamline showe
d that all design parameters have been realized.