J. Schreuer et al., A NEW SINGLE-CRYSTAL MOUNTING TECHNIQUE FOR LOW-BACKGROUND HIGH-TEMPERATURE X-RAY-DIFFRACTION, Journal of applied crystallography, 30, 1997, pp. 1162-1164
A new single-crystal mounting technique for high-temperature X-ray dif
fraction up to 1700 K on an imaging plate scanner has been developed.
The crystal is clamped mechanically by three to six very thin alumina
fibres. Besides the cheap and easy manufacturing procedure, its major
advantage is the resultant very low background; it consists mainly of
weak, smooth Debye-Scherrer rings which can be easily removed by image
-processing methods.