G. Moulard et al., IMPROVEMENT OF THE CANTILEVER BEAM TECHNIQUE FOR STRESS MEASUREMENT DURING THE PHYSICAL VAPOR-DEPOSITION PROCESS, Journal of vacuum science & technology. A. Vacuum, surfaces, and films, 16(2), 1998, pp. 736-742
Citations number
35
Categorie Soggetti
Physics, Applied","Materials Science, Coatings & Films
An improvement of an optical method for in situ measurement of the int
rinsic stress in thin films is described. The method presented is base
d on the well-known beam bending technique using the deflection of a l
aser beam that reflects itself on a sample. The first new development
lies in the evaluation of the bending plate equation. The second uses
image processing to determine the deformation of the sample. The metho
d has been applied to pure chromium films on glass substrates to valid
ate the stress measurements. The reproducibility of stress measurement
is of about 8%. Results show the great adaptability of the technique
to any kind of stress evolution during the physical vapor deposition p
rocess and give additional information about the evolution of stress v
ersus film thickness, in comparison with ex situ techniques, Finally,
a correlation between stress measurement and microstructure has been c
arried out. (C) 1998 American Vacuum Society.