The goal of the work was to develop a technique for preparing cantilev
ers for atomic force microscopy with ultra-sharp, ultra-hard tips. For
this purpose, two technologies were combined: (a) preparation of Si c
antilevers with the principal (111)-oriented face; (b) formation of th
e probe by growing of single-crystal Si columns on the cantilevers fro
m the vapor phase (vapor-liquid-solid VLS) with subsequent sharpening,
deposition of diamond on the tips formed, and sharpening of the diamo
nd tips by ion-beam bombardment. Sharp diamond tips with curvature rad
ii as small as 20 nm were formed.