A. Bosseboeuf et al., CHARACTERIZATION OF W FILMS ON SI AND SIO2 SI SUBSTRATES BY X-RAY-DIFFRACTION, AFM AND BLISTER TEST ADHESION MEASUREMENTS/, Microscopy microanalysis microstructures, 8(4-5), 1997, pp. 261-272
Contrary to most classical adhesion test, the blister test provides qu
antitative adhesion energy measurements. We demonstrate its applicatio
n to 1 mu m thick W films in tensile stress state deposited by xenon D
C magnetron sputtering on PECVn/Si(100) substrates. The W films surfac
e morphology; structure and residual stress were also characterized by
atomic force microscopy, X-ray diffraction and substrate curvature me
asurements as function of the deposition pressure. Films characteristi
cs are compared with those of W films deposited directly on Si(100) su
bstrates.