InP/GaAs(1 0 0) heterostructures grown by gas-source molecular-beam ep
itaxy were analyzed using three-beam bragg-surface diffraction (BSD) o
f the X-ray multiple diffraction (MD) phenomenon. The angular MD condi
tion is scanned by varying both, the omega incidence angle and the phi
rotation angle around [1 0 0] in order to provide the mapping of this
condition. From the two-dimensional mapping -omega:phi scan, the crys
talline perfection (mosaic spread) parallel (eta(phi)) and perpendicul
ar (eta(omega)) to the growth direction can be investigated along the
layer surface and the substrate interface. The omega:phi scan of the 0
0 0, 2 0 0, 1 (1) over bar 1 1 BSD is used to analyze the growth proc
essing and post-growth annealing of InP/GaAs samples. The effect of va
rious defect-reduction tools on layer and substrate crystal quality is
also investigated. (C) 1998 Elsevier Science B.V. All rights reserved
.