22 samples of baby-milk, baby-food, mother's milk and cow's milk were
analysed for their content of phthalates. After separating the fat by
gel permeation chromatography the esters of the phthalic acid were sep
arated by gas chromatography and identified and quantified by mass spe
ctrometry: As internal standards Deuterium-labelled dibutyl- and dioct
ylphthalate were added. Analysing for 10 different phthalates only DBP
and DEHP were found in the samples with maximum-concentrations till 5
0 resp. 200 mu g/kg with a detection-limit of 10 mu g/kg food. The rel
atively narrow range of the measured values point to the ubiquitous pr
esence of these two components.