A REACTION CELL FOR IN-SITU STUDIES OF HYDROTHERMAL TITRATION

Authors
NORBY P CAHILL C KOLEDA C PARISE JB
Citation
P. Norby et al., A REACTION CELL FOR IN-SITU STUDIES OF HYDROTHERMAL TITRATION, Journal of applied crystallography, 31, 1998, pp. 481-483
Citations number
9
Categorie Soggetti
Crystallography
Journal title
Journal of applied crystallography → ACNP
ISSN journal
00218898
Volume
31
Year of publication
1998
Part
3
Pages
481 - 483
Database
ISI
SICI code
0021-8898(1998)31:<481:ARCFIS>2.0.ZU;2-V
Abstract
A reaction cell for in situ studies of both ion-exchange and hydrother mal titration reactions has been designed and built. This cell allows the injection of reagents into a reaction mixture over time during X-r ay data collection. A demonstration experiment followed the injection of Na2SO4(aq) into BaCl2(aq) to yield a time-resolved X-ray powder dif fraction pattern of the precipitation of BaSO4(s).