Da. Collins et al., REAL-TIME EXTRACTION OF GROWTH-RATES FROM ROTATING SUBSTRATES DURING MOLECULAR-BEAM EPITAXY, Journal of vacuum science & technology. B, Microelectronics and nanometer structures processing, measurement and phenomena, 13(5), 1995, pp. 1953-1959
We present a method for measuring molecular-beam epitaxy growth rates
in near real-time on rotating substrates. This is done by digitizing a
video image of the reflection high-energy electron diffraction screen
, automatically tracking and measuring the specular spot width, and us
ing numerical techniques to filter the resulting signal. The digitizat
ion and image and signal processing take approximately 0.4 a to accomp
lish, so this technique offers the molecular-beam epitaxy grower the a
bility to actively adjust growth times in order to deposit a desired l
ayer thickness: The measurement has a demonstrated precision of approx
imately 2%, which is sufficient to allow active control of epilayer th
ickness by counting monolayers as they are deposited. When postgrowth
techniques, such as frequency domain analysis, are also used, the refl
ection high-energy electron diffraction measurement of layer thickness
on rotating substrates improves to a precision of better than 1%. Sin
ce all of the components in the system described are commercially avai
lable, duplication is straightforward. (C) 1995 American Vacuum Societ
y.