H. Nonaka et al., IN-SITU OBSERVATION OF GROWING SURFACE OF OXIDE-FILMS BY REFLECTION HIGH-ENERGY ELECTRON-DIFFRACTION BEAM EXCITED AUGER-ELECTRON SPECTROSCOPY, Journal of vacuum science & technology. A. Vacuum, surfaces, and films, 11(5), 1993, pp. 2676-2680
The reflection high-energy electron diffraction beam excited Auger ele
ctron spectroscopy (AES) was applied to in situ and real time observat
ion of the growing surface of films during molecular-beam epitaxy depo
sition. A compact electron energy analyzer assembly which consists of
an einzel lens, sector-type energy analyzer, microchannel plate detect
or, and magnetic shielding case was built to enable the measurement cl
ose to the substrate without disturbing the deposition. The system was
checked by the in situ AES measurement of crystals surface during cle
aning with ozone. The technique is applicable to analyze in situ the g
rowing surface of more complicated materials such as oxide superconduc
tors whose microstructures at an atomic level must be well controlled
for better quality and for use in microelectronic devices such as the
Josephson junction.