Wm. Duncan et al., HIGH-SPEED SPECTRAL ELLIPSOMETRY FOR IN-SITU DIAGNOSTICS AND PROCESS-CONTROL, Journal of vacuum science & technology. B, Microelectronics and nanometer structures processing, measurement and phenomena, 12(4), 1994, pp. 2779-2784
Real-time sensors are key for flexible manufacturing environments wher
e variable layer structures are processed concurrently. We have develo
ped a high speed spectral ellipsometer capable of precisely measuring
thicknesses and compositions of multilayer structures in situ and in r
eal-time (i.e., the time frame of process changes or about one second)
. This spectral ellipsometer has been integrated into several vacuum c
hambers of a flexible process flow. Utilizing phase modulation, multic
hannel detection, and digital signal processing techniques, less than
0.5 s is required for acquisition of 46 spectral points. Fast numerica
l algorithms and processor are used for reducing measured spectral ell
ipsometric data to physical parameters (i.e., thicknesses and composit
ions), in real time based on a ''standard model'' approach. Implementa
tions of spectral ellipsometric sensing in rapid thermal oxidation and
remote plasma etch are described. For thermally activated processes s
uch as oxidation, temperature dependent dielectric functions have been
employed for analyzing samples at process temperatures as high as 110
0-degrees-C. Multilayer combinations Of Si3N4, SiO2, Si3N4 plus SiO2 m
ixtures, and polycrystalline Si have been monitored and thicknesses co
ntrolled.