The growth defects in flux-grown NdxY1-xAl3(BO3)(4) (NYAB) single crys
tals have been investigated by means of chemical etching and synchrotr
on radiation techniques. The band-shaped and polysynthetic twins were
detected by optical microscopy due to the difference in etching rates
between the host crystal and the twin. In the meantime, the orientatio
n and symmetry of the twins were analyzed from their etching patterns.
A large number of etch pits with regular shapes were also found on th
e surface, and these etch pits correspond to outcrops of the dislocati
ons originating from the seed crystal or inclusions.