G. Abadal et al., A NEW METHOD TO PERFORM IN-SITU CURRENT-VOLTAGE CURVES WITH AN ELECTROCHEMICAL SCANNING TUNNELING MICROSCOPE, Ultramicroscopy, 66(3-4), 1996, pp. 133-139
A new method to perform in situ current voltage curves with an electro
chemical scanning tunneling microscope under bipotentiostatic control
is presented. The method eliminates the effect of (a) high parasitic c
apacitances that are present when tip and sample are immersed in a liq
uid and (b) electrochemical currents due to the effect of a polarizati
on out of the usual tip versus electrolyte voltage window. Several app
lications to the study of silicon surfaces in HF solutions are shown.