C. Liu et al., ION-BEAM-INDUCED SURFACE MODIFICATION OF CHEMICAL-VAPOR-DEPOSITION DIAMOND FOR X-RAY-BEAM POSITION MONITOR APPLICATIONS, Journal of vacuum science & technology. A. Vacuum, surfaces, and films, 15(3), 1997, pp. 1200-1205
Citations number
21
Categorie Soggetti
Physics, Applied","Materials Science, Coatings & Films
The Advanced Photon Source at Argonne National Laboratory is a third-g
eneration synchrotron facility that generates powerful x-ray beams on
its undulator beamlines for a variety of scientific and industrial use
r research programs. It is very important to know the position and the
angle of the x-ray beam during experiments. Due to very high heat flu
x levels, several patented x-ray beam position monitors (XBPMs) exploi
ting beneficial characteristics of chemical vapor deposition (CVD) dia
mond have been developed. These XBPMs have a thin layer of low-atomic-
mass metallic coating so that photoemission from the x rays generates
a minute but measurable current for position determination. Another co
ncept has been the graphitization of the CVD diamond surface to create
a very thin, intrinsic conducting layer that can stand much higher te
mperatures and have minimal x-ray transmission losses compared to coat
ed metallic layers. In the present study, a laboratory sputter ion sou
rce was used to transform selected surfaces of a CVD diamond substrate
into graphite. The effect of 1-5 keV argon ion bombardment on CVD dia
mond surfaces at various target temperatures from 200 to 500 degrees C
was studied using Auger electron spectroscopy and in situ electrical
resistivity measurements. Graphitization after the ion bombardment was
confirmed, and optimum conditions for graphitization were studied. Ra
man spectroscopy was applied to identify the overall diamond structure
in the bulk of CVD diamond substrate after the ion bombardments. It w
as found that the target temperature plays an important role in the st
ability and electrical conductivity of the irradiated CVD diamonds. (C
) 1997 American Vacuum Society.