Results are presented to show an improved method for composition chara
cterization of HgCdTe heterostructure using secondary ion mass spectro
scopy. This method utilizes the molecular ions CsM+ rather than M+/- i
ons. The advantage is that the molecular CsM+ ion yield, unlike the at
omic M+/- ions, is quite insensitive to the matrix material from which
they are emitted. Composition of multilayer HgCdTe structure can be d
etermined with excellent accuracy and depth resolution, Layer thicknes
s of HgCdTe heterostructure can also be calibrated.