ENERGY-FILTERED LORENTZ MICROSCOPY

Citation
J. Dooley et M. Degraef, ENERGY-FILTERED LORENTZ MICROSCOPY, Ultramicroscopy, 67(1-4), 1997, pp. 113-131
Citations number
20
Categorie Soggetti
Microscopy
Journal title
ISSN journal
03043991
Volume
67
Issue
1-4
Year of publication
1997
Pages
113 - 131
Database
ISI
SICI code
0304-3991(1997)67:1-4<113:ELM>2.0.ZU;2-5
Abstract
Energy-filtered Lorentz microscopy (EFLM) combines a post-column energ y filter with a high-resolution TEM, operated with the main objective lens switched off. In this paper we use a magnetostrictive material, T erfenol-D (Tb0.73Dy0.27Fe1.95), to illustrate the benefits of zero-los s filtering on both standard and coherent Fresnel and Foucault modes. It is shown that the signal-to-noise ratio of Foucault images is impro ved by an order of magnitude. We present a detailed study of magnetic domain configurations in the vicinity of growth twins and show that th e magnetic resolution of the system is better than 5 nm. Our observati ons compare favorably with micromagnetic models. We also show that mag netic induction mapping becomes a viable technique in thicker regions when the inelastically scattered electrons have been removed from the images. Finally, we present simulations of Fresnel and Foucault images , assuming two-dimensional periodic boundary conditions for the comput ation of the Aharonov-Bohm phase shift.