In this letter, we proposed a method in which a n-type GsAs wafer was
first anodized in HF for a short time to form a high density of etch p
its on its surface and then anodized in KOH solution to form a high de
nsity of pores with uniform distribution in it. Scanning electron micr
oscopy revealed feature sizes of the porous structure in the nanometer
range. The porous GaAs has been investigated using double crystal X-r
ay diffraction technique. Crystal quality and crystallographic orienta
tion of the porous layer were similar to those of the substrate. The l
attice constant of porous layer is slightly larger than that of the su
bstrate in the growth direction.